Test specimens machined at LTIDestructive testing is performed to evaluate physical characteristics of materials, such as strength, ductility, hardness and composition, and to determine susceptibility to corrosion. The information is most often used in material selection or failure analysis. This testing is performed on samples of material known as specimens or coupons that are prepared by machining to exacting dimensions and other precise requirements.

The Process

The four main processes performed in the production of test specimens are sawing, milling, turning and grinding. Although sawing is the starting point for all specimens, one or more of the other three processes may be performed during the preparation of specific types of specimens.

Sawing
Specimens are rough cut to length by sawing from a specific location on the sample material or part, as stated in a required specification or dictated in a drawing provided with the order. During this step, the material is cut into a workable size, which is generally close in size to the final specimen. If welds are involved, parts may be etched to identify position of the center line or heat-affected zone.

Turning
Turning test specimensTurning is performed on a lathe by rotating a part against a stationary cutting tool to center and turn in diameter. This is a required step for all round specimens including tensile, stress rupture, gleeble, jominy, rotating beam and fatigues, since rough-cut specimens are usually square in shape. In addition to further refining specimen dimensions, the turning process reduces the gage length and threads the ends when required by fixturing on test machines.

Milling
Milling Test SpecimensMilling is the process of cutting away material by feeding a work piece past a rotating cutter with multiple teeth. The machined surface may be flat, angular, or curved and can be milled to any combination of shapes. Specimens such as flat tensile, stress rupture, and hardness samples are precision machined by this process. Also, side, face and root bend specimens for weld qualifications and certain corrosion specimens are milled. Milling is also used to further refine charpy specimens for the next step, grinding.

Grinding
Grinding test specimensGrinding is the finish step for many types of specimens including charpy, hardness, compact tension and macro specimens used in metallurgical examinations. During grinding, a rotating abrasive wheel smooths the surface to give the material a refined look or to attain the desired finish. When required, this process can be used to create a high-quality surface finish to 32 Ra (roughness average) or better.

Machining at LTI

The Machine Shop at LTI prepares all types of test specimens to required ASTM specifications and customer requirements for mechanical and corrosion testing. Our machinists also rough cut and grind metallography specimens, prepare chips for ICP analysis and perform electrical discharge
machining (EDM). Most specimens are machined from metals, including metal matrix composites, hardened steels and nickel-base alloys, using the latest CNC turning, milling and grinding machines.

All machining is PRI/Nadcap accredited and LTI is on the NIST Qualified Manufacturers List for Charpy V-notch Impact verification specimens. Traceability of sample material and specimens is insured from receipt inspection through the final process.

LTI specimen machining is a time-saving convenience for testing customers. These services also are available to companies that perform testing inhouse. Refer to our Sample Size Guidelines when ordering.

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Polymer Testing Compliments Metal Testing Services

The range of materials testing services performed by Laboratory Testing Inc. has grown with the addition of Hardness Testing, Scanning Electron Microscopy (SEM) and Fourier Transform Infrared Spectroscopy (FTIR) for testing polymers such as plastic and rubber. These services complement the laboratory’s full-service metals testing capabilities and our materials analysis services that are also available for powdered metals, ores, ferroalloys, composites and ceramics.

The need for testing polymeric materials continues to grow as many industries, including aerospace, military and medical, continue to look for stronger, more reliable and less expensive materials to use in their component parts and devices. Laboratory Testing Inc. works with many customers in these industries, therefore, expansion into polymer testing was a convenient addition to our “one-stop” laboratory’s materials testing services. The services currently available provide information on material properties, characteristics and composition.

Scanning Electron Microscopy

Scanning electron microscopy or SEM analysis uses magnification and digital imaging to assist in evaluating polymers, metals and other materials for failure analysis, properties and characteristics. The SEM produces high resolution images at magnifications from 5x to 300,000x to aid in tests such as fractography, chemical attack, and particulate evaluation.

Fourier Transform Infrared Spectroscopy

FTIR analysis is an analytical technique used to identify organic, and in some cases, inorganic materials. The spectrometer used in FTIR analysis creates an absorption spectra with absorbance peaks that provide information about the chemical bonds and molecular structure of the test material. The data can be used to identify the general type of material under analysis by comparing the analytical spectrum with cataloged reference spectra to identify base polymers and additives.

Hardness Testing

LTI measures the hardness of polymers using the Shore Durometer Test to ASTM D2240. A material’s hardness is determined by its resistance to indentation when an indenter in the equipment penetrates the test sample. A variety of indenters are used when testing different types of materials from elastomers to rigid plastics.

More information on polymer testing is available from our Sales/Customer Service Department at sales@labtesting.com or 800-219-9095.

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Metals Testing and Certified Test Reports

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When is Ultrasonic Testing the NDT service of choice?

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When is Failure Analysis Performed?

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Defining Metallography

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X-ray Inspection for Detecting Flaws

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